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9mm 2ml Wide Opening Screw Vials If only a limited volume of sample is available, you will have to choose between using an insert for your regular autosampler vial, a microvial or a high recovery vial. Note: Most 12x32 mm autosampler vials hold between 1.5mL to 2.0mL of liquid, depending on where the manufacture measures the vial full. What minimum volume of sample should be in a HPLC vial (2ml Wit normal 2mL vials I would recomend between 150 and 250µL. My question is I prepare 2 ml of my...